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- Contents
- Table of Contents
- Bookmarks
Table of Contents
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Table of Contents
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Initial Operation
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Installation of the Control Software HT2 STD
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Connecting the Hydrotracer
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Measuring Principle
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The Reagent
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Performing a Test
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The Procedure Step by Step
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Selection of Temperature
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Selection of Sample Weight
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Using the Serial Balance
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Operation Menu with Manual Input: Loading the Hydrotracer
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Operation Menu with Automatic Weight Input: Loading the Hydrotracer
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Influence of the Filling Procedure on the Accuracy of the Test
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Measuring Period
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End of the Test
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Output of the Results and Storage
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HTML-Report
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PDF-Report
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Menu: Operator List
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Menu: List of Materials
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Cleaning the Reactor Interior
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Dry Run
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Errors
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Remarks Concerning Calcium Hydride
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HydroTracer
Operation Manual
aboni GmbH für Mess- und Automatisierungstechnik
aboni
FLV HT2
Version HT2 STD
Friedrich-Ebert-Str. 27
D-14548 Schwielowsee- Caputh
Tel.:
+49 700 abonifon
+49 700 22664 366
Fax:
+49 700 abonifax
+49 700 22664 329
E-Mail: info@aboni.de
Web:
www.aboni.de
16/01/2019
Table ofContents
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Table of Contents
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Summary of Contents for aboni HydroTracer FLV HT2
- Page 1 HydroTracer FLV HT2 Operation Manual Version HT2 STD 16/01/2019 aboni GmbH für Mess- und Automatisierungstechnik Friedrich-Ebert-Str. 27 D-14548 Schwielowsee- Caputh Tel.: +49 700 abonifon +49 700 22664 366 Fax: +49 700 abonifax +49 700 22664 329 E-Mail: info@aboni.de Web:...
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Page 3: Table Of Contents
Table of Contents Initial Operation ....................... 3 Installation of the Control Software HT2 STD ............3 Connecting the HydroTracer ................5 Measuring Principle ................... 6 The Reagent ..................... 7 Performing a Test ....................8 The procedure step by step ................8 Selection of Temperature ................. -
Page 5: Initial Operation
Initial Operation Initial Operation The HydroTracer is controlled by a PC and the signals from the instrument are analysed by the PC software. The data transmission occurs via USB-Port. Before first operation, the control program and the driver must be installed Installation of the Control Software HT2 STD Insert the DVD and start the installation by running the setup.exe within the directory [CD/DVD]: \HT2 STD\Volume... - Page 6 Initial Operation This mask appears. recommended not to change the settings. Click "Next >>" Now click on the field "I accept the license agreements", then on the field "Next >>" This mask appears. Click "Next >>"...
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Page 7: Connecting The Hydrotracer
Initial Operation This mask appears. Click "Next >>" In the Windows© Device Manager, a new entry "USB serial port" appears under the "Ports (COM & LPT)" section when the HydroTracer is connected to the computer via USB cable. Connecting the HydroTracer Switch on your PC (if not done already). -
Page 8: Measuring Principle
Initial Operation Measuring Principle The patented method of the HydroTracer determines the absolute water content. The mass of the water is measured within the reactor. The percentage of moisture of the sample is calculated by division with the sample weight. 1 The test material is heated in the sample tray;... -
Page 9: The Reagent
Initial Operation Note: The air-hydrogen atmosphere does not react chemically, because the temperature is much lower than needed to supply the activation energy of the oxyhydrogen gas reaction. Even if it would react, the theoretic maximum of the reaction enthalpy (the amount of energy which would be set free by the reaction of hydrogen with the oxygen of the air) is about 0.1 kJ and therefore harmless. -
Page 10: Performing A Test
Performing a Test Performing a Test Take care the accessories are within reach. Do not leave your sample material exposed to the ambient air over a longer period, especially if it is hydroscopic. Note: It is recommended to acquaint oneself with the operation before doing a „serious“ test. Therefore run the program and follow the menu until you have reached the step START / F10. - Page 11 Performing a Test Then select a location on your PC where you want to store the measurement results and reports. Then the software is ready for operation and the following main menu appears: (A) „Quit“-Button closes the application (B) „Settings"-Button opens the menu" Settings "(see „4.1 Menu: Settings & Company logo“) (C) Information display of available or connected serial devices (D) Status indicator for the HydroTracer (see „4.4 Status Display &...
- Page 12 Performing a Test After pressing the "Start" button, these input masks 1 appears: (A) Selection field of existing operators (B) Selection field of existing materials (C) The checkbox "Use Standard operator?" is described in „4.2 Menu: Operator List“ (D) Comment field for entering additional notes on the current measurement -Button: Add a new operator or material -Button: Opens the Menu "Operator List"...
- Page 13 Performing a Test After selecting an operator and a material, a second input mask 2 appears: Display of the set parameters for the measurement opens a tool for determining the sample weight (see Pressing section „2.3 Selection of Sample Weight“) Comment field Checkbox for connecting a serial scale (if a scale is connected) If a hook is set here, the program automatically opens an HTML report after the...
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Page 14: Selection Of Temperature
Performing a Test Selection of Temperature The temperatures given in the materials table are proposals, which might not fit always for each member of a group of materials. Generally a temperature is chosen which is as high as possible to accelerate the evaporation of water but low enough to avoid thermal decomposing. Usually the melting of the sample should be avoided to allow easier cleaning of the sample tray. - Page 15 Performing a Test For an explanation, an example: Selecting the selection field (A) opens a list of relative water contents according to the following figure: An expected water content of 0.01% is selected. When pressing button (B) the permissible and, if necessary, the optimal water content is calculated. The result of the calculation is shown in the following figure: The permissible weight must not be less than 2 gram and not greater than 90 gram.
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Page 16: Using The Serial Balance
Performing a Test Using the serial balance The connection of the serial scale with the software can be done in several ways: A) Before starting the software HT2 STD connect the PC and the scale with the serial cable and switch on the scale. Start the software HT2 STD. -
Page 17: Operation Menu With Manual Input: Loading The Hydrotracer
Performing a Test Operation menu with manual input: Loading the HydroTracer This chapter describes the steps of the manual operation as shown on the screen. The pictures clarify the action momentarily needed. Below the picture this action is described shortly. The panel counting down the number on the right indicates the remaining time in seconds. - Page 18 Performing a Test Lift the reagent tray with the pincers and Take a 1/3 of a spoon with the spatula remove the used reagent. and fill it into the reagent tray. Take out the sample tray by lifting it slightly and pull it out off the front.
- Page 19 Performing a Test Remove the sample tray and dispose the Fill in the sample material. Enter the sample material of the former test. Place weight in grams. Click on “Continue”. the sample tray on the balance and tare Clean the rim with the brush. Insert the sample tray.
- Page 20 Performing a Test Insert the reagent tray with the pincers. Clean O-ring and seal face of with the brush Close reactor lid. Take care the clasp is Push down simultaneously the side properly locked. handles. The system fan must run again.
- Page 21 Performing a Test After 99 seconds the CONTINUE button appears. The handling steps are displayed in case further assistance is needed. Click start measurement. further action required by the operator...
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Page 22: Operation Menu With Automatic Weight Input: Loading The Hydrotracer
Performing a Test Operation menu with automatic weight input: Loading the HydroTracer The menu with a connected balance is quite similar to the manual weight input menu. Below are shown the deviations to the manual input of the weight. Place the sample tray on the weighing Transfer the weight data from the balance plate and tare. -
Page 23: Influence Of The Filling Procedure On The Accuracy Of The Test
Performing a Test Influence of the filling procedure on the accuracy of the test During the filling procedure the decline hydrogen concentration is detected. This decline is used by the software to detect the minimum sensor signal (signal at zero hydrogen content). This value is subtracted from the signal value obtained during the test. -
Page 24: Measuring Period
Performing a Test Measuring period Now the sample is heated to the selected temperature. The current heating temperature is shown in the digital display (F). In the diagram (G) the current total amount of water is shown in [mg]. That means both the amount of water from the sample and the amount of water from the ambient air introduced during the filling procedure are displayed. -
Page 25: End Of The Test
Performing a Test End of the test At the end of the measurement, a selection menu appears (see (E) „2.8 Measuring period“), whether the measurement should be saved or discarded. If no selection is made within 5 seconds, the measurement is saved automatically. After saving, the measurement results are displayed as HTML-Report according to “3.1 HTML- Report”. -
Page 26: Output Of The Results And Storage
"HT-TAB. txt", each report can be assigned in the table. The container file contains the report as PDF file and a binary data file with the extension ". t". The latter is used for support and remote fault diagnosis by aboni GmbH. -
Page 27: Html-Report
Output of the results and storage HTML-Report If a checkmark has been set in the CheckBox "Show test Report" in Input mask 2 (see „2.1 The procedure step by step“) a measurement report is opened in the Web browser after a measurement has been completed: The HTML test report contains all the information provided by the user, the measurement results and information about the location and the software version. -
Page 28: Pdf-Report
Menu: Settings & Company logo”), an additional report is created in the desired language. Furthermore you have the possibility to insert a company logo into the report (cf. company logo "aboni" in the picture above). The insertion of a company logo is explained in „4.1 Menu: Settings & Company logo “. -
Selection Menus & Status Display Selection Menus & Status Display Menu: Settings & Company logo After calling up the menu "settings" from the main screen, this window appears: (A) Press to open the menu „List of materials“ (B) Press to open the menu „Operators List” (C) Selection of program language (D) Display HTML report after measurement (hook: yes, empty: no) (E) Create a test report in a second language (hook: yes, empty: no)
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Page 30: Menu: Operator List
Selection Menus & Status Display (G) Place the hook in the checkbox and connect the PC and the scale with the serial cable and switch on the scale. Then press the "Connect" button and the software will connect the scale. You get the info window as in „2.4 Using the serial balance“ described. The current storage path of the test reports. -
Page 31: Menu: List Of Materials
Selection Menus & Status Display With the button "Edit" the selected operator can be edited. The "Close" button exits the menu. Menu: List of materials Explanation of the functions within the “List of materials". The material list already contains a variety of materials, indicating the density and recommended heating temperature. -
Selection Menus & Status Display Status Display & Information field In the main menu (cf. „2.1 The procedure step by step“ field „(C)“ and „(D)“) you get information about the connection of the HydroTracer (and the serial scale), as well as a status message about the HydroTracer itself.
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Page 33: Cleaning The Reactor Interior
Cleaning the reactor interior Cleaning the reactor interior Sometimes volatiles are set free during the measurement, e.g. softeners and waxes. These substances will condense on the cooler inner surfaces of the reactor depending on condensing temperature and heating temperature. It may be necessary to clean the reactor sometimes, if visible layers occur. -
Page 34: Dry Run
Dry Run If the reagent was dispersed involuntary in the whole reactor, it is also recommended to clean the reactor. If the powder is only below the reagent tray in some quantities, just pull out the cables, open the reactor, take out reagent tray and sample tray, turn the instrument on the top and let the powder fall out. -
Page 35: Errors
Errors Errors If an error occurs during the communication between Hydrotracer and PC, the HydroTracer sends an error message to the software. In some cases, this will interrupt the measurement. Following table shows the possible errors: Code Error Reactor Heater Door Contact Reactor PT1000 Mainboard (PTC3) BME280 –... -
Page 36: Remarks Concerning Calcium Hydride
Remarks concerning calcium hydride Remarks concerning calcium hydride Calcium hydride is reported as dangerous goods in the material safety data sheet. This classification refers to large amounts, so that the recommended precautions to exposure are valid over any length of time with any great amount (e.g. filling a silo or the like) About the toxicity of calcium hydrid: Calcium hydride reacts with water immediately to calcium hydroxide (slaked lime) and hydrogen. - Page 37 CE- Konformitätserklärung / CE Declaration of Conformity Die Firma / The manufacturer aboni GmbH für Mess- und Automatisierungstechnik Anschrift/Address: Friedrich-Ebert-Str. 27, 14548 Schwielowsee, Deutschland / Germany Telefon/Phone: ++49(0)700 22664 366 Fax: ++49(0)700 22664 329 Web: www.aboni.de E-Mail: info@aboni.de erklärt hiermit, dass die Produkte / hereby declares that the following products...
- Page 38 SAFETY DATA SHEET according to Regulation (EC) No. 1907/2006 CaH2 Typ K 0-2 mm - Lager Version: 2.2 Revision Date 10.03.2017 Print Date 23.03.2018 SECTION 1: Identification of the substance/mixture and of the company/undertaking 1.1 Product identifier Trade name : CaH2 Typ K 0-2 mm - Lager 1.2 Relevant identified uses of the substance or mixture and uses advised against Use of the Substance/Mixture : Reducing agents, Alloy component., Pyrotechnics.
- Page 39 SAFETY DATA SHEET according to Regulation (EC) No. 1907/2006 CaH2 Typ K 0-2 mm - Lager Version: 2.2 Revision Date 10.03.2017 Print Date 23.03.2018 Precautionary statements Prevention: P231 + P232 Handle and store contents under inert gas. Protect from moisture. P280 Wear protective gloves/ protective clothing/ eye protection/ face protection.
- Page 40 SAFETY DATA SHEET according to Regulation (EC) No. 1907/2006 CaH2 Typ K 0-2 mm - Lager Version: 2.2 Revision Date 10.03.2017 Print Date 23.03.2018 General advice : First Aid responders should pay attention to self-protection and use the recommended protective clothing Take off contaminated clothing and shoes immediately.
- Page 41 SAFETY DATA SHEET according to Regulation (EC) No. 1907/2006 CaH2 Typ K 0-2 mm - Lager Version: 2.2 Revision Date 10.03.2017 Print Date 23.03.2018 Further information : Use water spray to cool unopened containers. Be aware of a dangerous reaction with water, if the container is ruptured.
- Page 42 SAFETY DATA SHEET according to Regulation (EC) No. 1907/2006 CaH2 Typ K 0-2 mm - Lager Version: 2.2 Revision Date 10.03.2017 Print Date 23.03.2018 7.2 Conditions for safe storage, including any incompatibilities Requirements for storage : Keep under argon. areas and containers Store in original container.
- Page 43 SAFETY DATA SHEET according to Regulation (EC) No. 1907/2006 CaH2 Typ K 0-2 mm - Lager Version: 2.2 Revision Date 10.03.2017 Print Date 23.03.2018 Protective gloves have to be replaced at the first sign of dete- rioration. Eye protection : Tightly fitting safety goggles Eye protection (EN 166) Skin and body protection : Flame retardant antistatic protective clothing.
- Page 44 SAFETY DATA SHEET according to Regulation (EC) No. 1907/2006 CaH2 Typ K 0-2 mm - Lager Version: 2.2 Revision Date 10.03.2017 Print Date 23.03.2018 Molecular weight 42.10 g/mol No data available Melting point/ range 816.0 °C Decomposition temperature 600 °C Sublimation point No data available Vapour pressure...
- Page 45 SAFETY DATA SHEET according to Regulation (EC) No. 1907/2006 CaH2 Typ K 0-2 mm - Lager Version: 2.2 Revision Date 10.03.2017 Print Date 23.03.2018 Hazardous reactions : In contact with water releases flammable gases which may ignite spontaneously. Dust can form an explosive mixture in air. Dangerous reaction with water, acids and oxidising substanc- es to form flammable gases.
- Page 46 SAFETY DATA SHEET according to Regulation (EC) No. 1907/2006 CaH2 Typ K 0-2 mm - Lager Version: 2.2 Revision Date 10.03.2017 Print Date 23.03.2018 SECTION 12: Ecological information 12.1 Toxicity Toxicity to fish : No data available 12.2 Persistence and degradability Biodegradability : The methods for determining biodegradability are not applica- ble to inorganic substances.
- Page 47 SAFETY DATA SHEET according to Regulation (EC) No. 1907/2006 CaH2 Typ K 0-2 mm - Lager Version: 2.2 Revision Date 10.03.2017 Print Date 23.03.2018 IATA 1404 14.2 UN proper shipping name : CALCIUM HYDRIDE : CALCIUM HYDRIDE : CALCIUM HYDRIDE IMDG : Calcium hydride IATA...
- Page 48 SAFETY DATA SHEET according to Regulation (EC) No. 1907/2006 CaH2 Typ K 0-2 mm - Lager Version: 2.2 Revision Date 10.03.2017 Print Date 23.03.2018 SECTION 15: Regulatory information 15.1 Safety, health and environmental regulations/legislation specific for the substance or mixture REACH - Candidate List of : This product does not contain substances of very high con- Substances of Very High...
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